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高效液相色谱法测定金胆片中龙胆苦苷的含量
Alternative TitleDetermination of Gentiopicroside in Jindan Tabletes by HPLC
葛卫红; 郭建友; 蔡金娜; 薛建国; 刘月庆
2006
Source Publication中国实验方剂学杂志
ISSN1005-9903
Volume12Issue:11Pages:010-012
Abstract目的:建立用高效液相色谱法(HPLC)测定金胆片中龙胆苦苷的含量测定方法。方法:采用YMC ODS(4.6mm×150mm,5μm)色谱柱,流动相为乙腈-水(11∶89),流速为1.0mL.min-1; 检测波长为274nm。结果:龙胆苦苷在0.106~1.277μg范围内呈良好的线性关系,r=0.999 9,平均回收率为98.73%,RSD为2.7%。结论:本方法简便可行,重复性好,能有效地控制金胆片成品的质量。
Keyword高效液相色谱法 龙胆苦苷 金胆片
Subject Area医学心理学 ; 医学心理学
Indexed By中文核心期刊要目总览 ASPT来源刊 CJFD收录刊
Language中文
NoteObjective:To develop a HPLC method for determination of gentiopicroside in Jindan tabletes.Methods:The separation was performed on YMC ODS(150×6mm,5μm)column with a mobile phase composed of acetonitrile-water(11∶89).The flow rate was 1.0mL·min~(-1).The detecting wavelength was 274nm.Results:The Calitration curve of gentiopicroside was in the range of 0.11~1.28μg,r=0.9999.The average recovery was 98.7% and RSD was 2.7%.Conclusion:The method is simple,rapid and accurate,and can be used for quality control of ...
Document Type期刊论文
Identifierhttp://ir.psych.ac.cn/handle/311026/3092
Collection中国科学院心理研究所回溯数据库(1956-2010)
Corresponding Author葛卫红
Recommended Citation
GB/T 7714
葛卫红,郭建友,蔡金娜,等. 高效液相色谱法测定金胆片中龙胆苦苷的含量[J]. 中国实验方剂学杂志,2006,12(11):010-012.
APA 葛卫红,郭建友,蔡金娜,薛建国,&刘月庆.(2006).高效液相色谱法测定金胆片中龙胆苦苷的含量.中国实验方剂学杂志,12(11),010-012.
MLA 葛卫红,et al."高效液相色谱法测定金胆片中龙胆苦苷的含量".中国实验方剂学杂志 12.11(2006):010-012.
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